1GOF

NOVEL THIOETHER BOND REVEALED BY A 1.7 ANGSTROMS CRYSTAL STRUCTURE OF GALACTOSE OXIDASE

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	98.000, 89.400, 86.700
Unit cell angles	90.00, 117.80, 90.00

Refinement procedure

Resolution	10.000 - 1.700
R-factor	0.177
RMSD bond length	0.018
RMSD bond angle	0.050 *
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.700 *	1.700 *
Rmerge	0.039 *
Total number of observations	117980 *
Number of reflections	57092 *	5908 *
Completeness [%]	79.1 *	52.6 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	acetate	0.80 (M)
2	1	reservoir	ammonium sulfate