1GLI

DEOXYHEMOGLOBIN T38W (ALPHA CHAINS), V1G (ALPHA AND BETA CHAINS)

Experimental procedure

Source type	ROTATING ANODE
Temperature [K]	300
Detector technology	DIFFRACTOMETER
Collection date	1993-08-10
Detector	ENRAF-NONIUS FAST
Spacegroup name	P 1 21 1
Unit cell lengths	63.150, 83.590, 53.800
Unit cell angles	90.00, 99.34, 90.00

Refinement procedure

Resolution	? - 2.500
R-factor	0.135 *
Structure solution method	MUTANT-NATIVE DIFFERENCE MAP STARTING MODEL FOR MOLECULAR REPLACEMENT: NULL
Data reduction software	MADNES
Data scaling software	CCP4

Data quality characteristics

	Overall
Low resolution limit [Å]	22.000
High resolution limit [Å]	2.480
Rmerge	0.096
Total number of observations	25572 *
Number of reflections	15560 *
Completeness [%]	76.5
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5 *		Perutz, M.F., (1968) J. Cryst. Growth, 2, 54. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	4 (M)
2	1	1		2 (M)
3	1	1		2 (M)