1GEC
GLYCYL ENDOPEPTIDASE-COMPLEX WITH BENZYLOXYCARBONYL-LEUCINE-VALINE-GLYCINE-METHYLENE COVALENTLY BOUND TO CYSTEINE 25
Experimental procedure
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 |
Unit cell lengths | 55.780, 55.780, 64.430 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.100 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.25800 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.900 * |
Data reduction software | MOSFLM |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.100 |
Rmerge | 0.050 |
Number of reflections | 14026 |
Completeness [%] | 97.4 |
Redundancy | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 5.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | glycyl endopeptidase | 21.7 (mg/ml) | |
2 | 1 | 1 | 3.2 (M) | ||
3 | 1 | 1 | sodium acetate | 50 (mM) |