1GCL
GCN4 LEUCINE ZIPPER CORE MUTANT P-LI
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1992 |
| Detector | RIGAKU RAXIS |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 47.432, 48.634, 51.765 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 2.100 |
| R-factor | 0.152 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 2.900 |
| Data reduction software | R-AXIS |
| Phasing software | X-PLOR |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.100 * |
| Rmerge | 0.070 * |
| Number of reflections | 5643 |
| Completeness [%] | 73.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 3 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | peptide | 10 (mg/ml) | |
| 2 | 1 | drop | sodium acetate | 100 (mM) | |
| 3 | 1 | drop | ammonium sulfate | 85 (mM) | |
| 4 | 1 | drop | PEG1400 | 10 (%) | |
| 5 | 1 | drop | isopropanol | 10 (%) | |
| 6 | 1 | reservoir | sodium acetate | 100 (mM) |
