1G88
S4AFL3ARG515 MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-01 |
Detector | RIGAKU |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 140.855, 140.855, 194.613 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.500 - 3.000 |
R-factor | 0.203 |
Rwork | 0.203 |
R-free | 0.26340 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.126 | 0.485 |
Total number of observations | 72845 * | |
Number of reflections | 19552 | |
<I/σ(I)> | 9.5 | 5.5 |
Completeness [%] | 97.9 | 88 |
Redundancy | 3.72 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 * | 298 | pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 2 | HEPES | 100 (mM) | |
2 | 1 | 2 | lithium sulfate | 250 (mM) | |
3 | 1 | 2 | PEG4000 | 10 (%(v/v)) |