1G2M

FACTOR XA INHIBITOR COMPLEX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	293
Detector technology	IMAGE PLATE
Collection date	1998-01-21
Detector	MARRESEARCH
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	57.400, 73.200, 79.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.510 - 3.020
R-factor	0.218 *
Rwork	0.218
R-free	0.27800
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.005 *
RMSD bond angle	1.530 *
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	CNX (2000)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	3.000
Rmerge	0.122
Total number of observations	54275 *
Number of reflections	6623
<I/σ(I)>	5.5
Completeness [%]	94.4
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *			Skrzypczak-Jankun, E., (1991) J. Mol. Biol., 221, 1379. *