1G0T
DSBC MUTANT C101S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.441, 78.501, 95.697 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.720 - 2.600 |
R-factor | 0.212 |
Rwork | 0.212 |
R-free | 0.27400 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.760 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.097 | 0.442 |
Number of reflections | 14441 | |
<I/σ(I)> | 23.8 | |
Completeness [%] | 99.0 | 94.1 |
Redundancy | 17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.9 | 291 | 23-25% PEG 550MME, 100mM Tris/HCl pH 8.9, VAPOR DIFFUSION, HANGING DROP, temperature 291K |