1FND

REFINED CRYSTAL STRUCTURE OF SPINACH FERREDOXIN REDUCTASE AT 1.7 ANGSTROMS RESOLUTION: OXIDIZED, REDUCED, AND 2'-PHOSPHO-5'-AMP BOUND STATES

Replaces:  2FNR

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	90.700, 57.700, 68.100
Unit cell angles	90.00, 100.00, 90.00

Refinement procedure

Resolution	9999.000 * - 1.700
R-factor	0.174
RMSD bond length	0.017
RMSD bond angle	2.500
Refinement software	TNT (5A)

Data quality characteristics

	Overall
High resolution limit [Å]	1.700 *
Rmerge	0.050 *
Total number of observations	95754 *
Number of reflections	37112 *
Completeness [%]	98.0 *
Redundancy	2.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	1.5 (M)
2	1	reservoir	McIlvain's buffer	0.2 (M)	sodium citrate-phosphate