1FLR

4-4-20 FAB FRAGMENT

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1988-10-21
Detector	SIEMENS-NICOLET X100
Spacegroup name	P 1
Unit cell lengths	42.750, 43.870, 58.170
Unit cell angles	95.15, 86.85, 98.01

Refinement procedure

Resolution	10.000 - 1.850
R-factor	0.188
RMSD bond length	0.017
RMSD bond angle	0.037
Data reduction software	XENGEN
Refinement software	PROFFT

Data quality characteristics

	Overall
High resolution limit [Å]	1.790 *
Rmerge	0.041
Total number of observations	76616 *
Number of reflections	29963
Completeness [%]	70.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *		15 *	Gibson, A.L., (1988) Proteins: Struct.,Funct., Genet., 3, 155. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	sodium phosphate	50 (mM)
2	1	1	protein	14-30 (mg/ml)
3	1	2	PEG3350	25-50 (%(w/v))