1FLP
STRUCTURE OF THE SULFIDE-REACTIVE HEMOGLOBIN FROM THE CLAM LUCINA PECTINATA: CRYSTALLOGRAPHIC ANALYSIS AT 1.5 ANGSTROMS RESOLUTION
Experimental procedure
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.970, 38.390, 42.650 |
| Unit cell angles | 90.00, 97.40, 90.00 |
Refinement procedure
| Resolution | 15.000 - 1.500 |
| R-factor | 0.17 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.700 |
| Phasing software | X-PLOR |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Rmerge | 0.061 * |
| Number of reflections | 17354 * |
| Completeness [%] | 90.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 4.8 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 20 (mg/ml) | |
| 2 | 1 | drop | acetate | 0.05 (M) | |
| 3 | 1 | drop | ammonium sulfate | 1.3 (M) | |
| 4 | 1 | reservoir | ammonium sulfate | 2.6 (M) |
