1FKX

MURINE ADENOSINE DEAMINASE (D296A)

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1993-05-02
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	C 1 2 1
Unit cell lengths	102.710, 94.070, 73.080
Unit cell angles	90.00, 127.27, 90.00

Refinement procedure

Resolution	8.000 - 2.400
R-factor	0.17 *
Rwork	0.158
RMSD bond length	0.012
RMSD bond angle	1.680 *
Data reduction software	SDMS (DETECTOR SYSTEM (NIELSEN))
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.042
Total number of observations	25228 *
Number of reflections	15662
Redundancy	1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	4.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	7 (mg/ml)
2	1	drop		50 (mM)
3	1	drop	sodium citrate	50 (mM)
4	1	drop	PEG6000	7.5 (%)
5	1	reservoir	PEG6000	15 (%)