1FKW
MURINE ADENOSINE DEAMINASE (D295E)
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1993-09-06 |
| Detector | XUONG-HAMLIN MULTIWIRE |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 102.840, 94.180, 73.240 |
| Unit cell angles | 90.00, 127.37, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.400 |
| R-factor | 0.176 |
| Rwork | 0.176 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.710 * |
| Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.400 * |
| Rmerge | 0.051 |
| Total number of observations | 40777 * |
| Number of reflections | 24014 |
| Redundancy | 1.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 4.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 7 (mg/ml) | |
| 2 | 1 | drop | 50 (mM) | ||
| 3 | 1 | drop | sodium citrate | 50 (mM) | |
| 4 | 1 | drop | PEG6000 | 7.5 (%) | |
| 5 | 1 | reservoir | PEG6000 | 15 (%) |
