1FKK

ATOMIC STRUCTURE OF FKBP12, AN IMMUNOPHILIN BINDING PROTEIN

Experimental procedure

Detector technology	IMAGE PLATE
Spacegroup name	P 43 21 2
Unit cell lengths	34.100, 34.100, 202.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 2.300 *
R-factor	0.158
Rwork	0.158
RMSD bond length	0.017
RMSD bond angle	1.900 *
Data reduction software	MANUFACTURER (SUPPLIED (MSC))
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.300 *
Rmerge	0.049 *
Total number of observations	10574 *
Number of reflections	3977 *
Completeness [%]	68.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	7.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	140 (mg/ml)
2	1	reservoir	sodium sulfate	1.4-1.6 (M)
3	1	reservoir	cacodylate	100 (mM)