1FIL
HUMAN PLATELET PROFILIN I CRYSTALLIZED IN HIGH SALT ACTIN-BINDING PROTEIN
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 290 |
| Detector technology | AREA DETECTOR |
| Collection date | 1993 |
| Detector | SIEMENS-NICOLET X100 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 75.050, 31.770, 62.820 |
| Unit cell angles | 90.00, 123.41, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.000 |
| Rwork | 0.191 |
| Structure solution method | MR |
| Starting model (for MR) | 1fil |
| RMSD bond length | 0.013 |
| RMSD bond angle | 0.031 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | X-PLOR |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.300 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.041 |
| Number of reflections | 8076 |
| <I/σ(I)> | 18.2 |
| Completeness [%] | 94.1 |
| Redundancy | 1.28 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.7 | CRYSTALLIZED FROM AMMONIUM SULFATE SOLUTION, pH 6.7 |
