1FIC

STRUCTURE OF HUMAN GAMMA FIBRINOGEN 30 KD CARBOXYL TERMINAL FRAGMENT

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1996-04-28
Detector	RIGAKU
Spacegroup name	H 3
Unit cell lengths	164.650, 164.650, 84.930
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.500
R-factor	0.171
Rwork	0.171
R-free	0.24400
RMSD bond length	0.010
RMSD bond angle	24.270 *
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Rmerge	0.083
Number of reflections	26495
Completeness [%]	89.2
Redundancy	2.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	6		stabilized in a Tris/NaCl solutioncontaining the inhibitor and then dialyzed against a 5 mM MES solution *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG3350	20 (%)
2	1	reservoir		70 (mM)
3	1	reservoir	Tris-HCl	0.1 (M)