1FIB
RECOMBINANT HUMAN GAMMA-FIBRINOGEN CARBOXYL TERMINAL FRAGMENT (RESIDUES 143-411) BOUND TO CALCIUM AT PH 6.0
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1995-09-11 |
Detector | SIEMENS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.530, 68.420, 47.670 |
Unit cell angles | 90.00, 105.36, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.100 |
R-factor | 0.159 |
Rwork | 0.159 |
R-free | 0.22700 |
RMSD bond length | 0.009 |
RMSD bond angle | 24.490 * |
Data reduction software | XENGEN |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.000 |
High resolution limit [Å] | 2.030 |
Rmerge | 0.033 |
Number of reflections | 12334 |
Completeness [%] | 82.7 |
Redundancy | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | or 18 % PEG8000 and 70 mM CaCl2 in 0.1M MES buffered at pH 6.0 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG3350 | (%) | |
2 | 1 | reservoir | (mM) |