1FAT

PHYTOHEMAGGLUTININ-L

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994-07-05
Spacegroup name	C 1 2 1
Unit cell lengths	106.300, 121.200, 90.800
Unit cell angles	90.00, 93.70, 90.00

Refinement procedure

Resolution	10.000 - 2.800
R-factor	0.2
Rwork	0.200
R-free	0.23000
RMSD bond length	0.017
RMSD bond angle	28.160 *
Data reduction software	MADNES
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Rmerge	0.099
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8.5 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG6000	8 (%(w/v))
2	1	reservoir	Tris	100 (mM)
3	1	drop	PEG6000	8 (%(w/v))
4	1	drop	Tris	100 (mM)
5	1	drop	PHA-L solution	5 (mg/ml)