1ERW
HUMAN THIOREDOXIN DOUBLE MUTANT WITH CYS 32 REPLACED BY SER AND CYS 35 REPLACED BY SER
Experimental procedure
Detector technology | DIFFRACTOMETER |
Collection date | 1995-04-20 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 67.770, 26.380, 51.640 |
Unit cell angles | 90.00, 95.08, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.800 |
R-factor | 0.21 |
Rwork | 0.210 |
R-free | 0.26000 |
RMSD bond length | 0.016 |
RMSD bond angle | 25.300 * |
Data reduction software | MADNES |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | |
High resolution limit [Å] | 1.800 | |
Rmerge | 0.044 | |
Total number of observations | 23947 * | |
Number of reflections | 7917 | |
Completeness [%] | 91.0 | 77 * |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 3.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | sodium acetate | 10 (mM) | |
2 | 1 | drop | MPD | 25 (%(v/v)) | |
3 | 1 | drop | dithiothreitol | 5 (mM) | |
4 | 1 | reservoir | sodium acetate | 10 (mM) | |
5 | 1 | reservoir | MPD | 50 (%(v/v)) | |
6 | 1 | reservoir | dithiothreitol | 5 (mM) |