1EAH

PV2L COMPLEXED WITH ANTIVIRAL AGENT SCH48973

Experimental procedure

Source type	SYNCHROTRON
Source details	CHESS BEAMLINE F1
Synchrotron site	CHESS
Beamline	F1
Detector technology	IMAGE PLATE
Collection date	1996-03
Detector	FUJI
Spacegroup name	C 2 2 21
Unit cell lengths	345.700, 497.200, 485.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.900
R-factor	0.185
Rwork	0.185
RMSD bond length	0.009
RMSD bond angle	26.700 *
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000 *
High resolution limit [Å]	2.900 *	2.900 *
Rmerge	0.110	0.227 *
Total number of observations	1242301 *
Number of reflections	444639 *
Completeness [%]	48.9 *	34.9 *
Redundancy	2.79

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	0.9-1.4 (%)
2	1	reservoir		100-250 (mM)
3	1	drop	virus	5 (mg/ml)