1DUR
Replacement for 1FDX 2(4FE4S) ferredoxin from (NOW) Peptostreptococcus asaccharolyticus
Replaces: 1FDXExperimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | OTHER |
| Temperature [K] | 298 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1972-01-01 |
| Detector | PICKER |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 30.520, 37.750, 39.370 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.14 |
| Rwork | 0.155 |
| Data reduction software | PICKER |
| Refinement software | X-PLOR (3.843) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.050 |
| Number of reflections | 3220 |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 7.5 | 277 | 3.3-3.5M ammonium sulfate, tris-chloride buffer, pH 7.5, EVAPORATION, temperature 277.0K |
