1DTX
CRYSTAL STRUCTURE OF ALPHA-DENDROTOXIN FROM THE GREEN MAMBA VENOM AND ITS COMPARISON WITH THE STRUCTURE OF BOVINE PANCREATIC TRYPSIN INHIBITOR
Experimental procedure
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 73.530, 39.060, 23.150 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 7.000 - 2.200 |
| R-factor | 0.169 |
| RMSD bond length | 0.027 |
| RMSD bond angle | 0.036 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.200 * |
| Rmerge | 0.079 * |
| Number of reflections | 3451 * |
| Completeness [%] | 96.5 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5.7 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein solution | 10 (mg/ml) | |
| 2 | 1 | drop | citrate | 50 (mM) | plus 0.003ml of the reservoir |
| 3 | 1 | reservoir | ammonium sulfate | 2.7 (M) | |
| 4 | 1 | reservoir | citrate | 50 (mM) | |
| 5 | 1 | reservoir | phenol | 20 (mM) |
