1DNV
PARVOVIRUS (DENSOVIRUS) FROM GALLERIA MELLONELLA
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 120 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-12 |
| Detector | FUJI |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 264.440, 264.440, 683.450 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 9.000 - 3.600 |
| R-factor | 0.271 |
| Rwork | 0.271 |
| Structure solution method | MOLECULAR REPLACEMENT AND NCS SYMMETRY AVERAGING |
| Starting model (for MR) | CRYO-EM RECONSTRUCTION |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.900 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | GLRF |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.000 | 3.580 |
| High resolution limit [Å] | 3.500 | 3.500 |
| Rmerge | 0.110 | 0.580 |
| Total number of observations | 164912 * | |
| Number of reflections | 107965 | |
| <I/σ(I)> | 10 | 1.5 |
| Completeness [%] | 35.6 | 15.2 |
| Redundancy | 1.5 | 1.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.5 | 4 * | pH 7.5 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PEG8000 | 5 (%) |
