1DN8
STRUCTURE OF A Z-DNA WITH TWO DIFFERENT BACKBONE CHAIN CONFORMATIONS. STABILIZATION OF THE DECADEOXYOLIGONUCLEOTIDE D(CGTACGTACG) BY (CO(NH3)6)3+ BINDING TO THE GUANINE
Experimental procedure
| Detector technology | DIFFRACTOMETER |
| Detector | ENRAF-NONIUS CAD4 |
| Spacegroup name | P 65 |
| Unit cell lengths | 17.930, 17.930, 43.410 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.500 |
| R-factor | 0.255 * |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.500 |
| Rmerge | NaN * |
| Number of reflections | 506 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 * | VAPOR DIFFUSION, temperature 279.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | PROPANOL | ||
| 3 | 1 | 1 | SPERMINE | ||
| 4 | 1 | 1 | [CO(NH3)6]CL3 | ||
| 5 | 1 | 2 | WATER | ||
| 6 | 1 | 2 | PROPANOL |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | deoxydecamer | 1.5 (mM) | ||
| 2 | 1 | spermine | 0.625 (mM) | ||
| 4 | 1 | reservoir | n-propanol | 30 (%(v/v)) |
