1DM0
SHIGA TOXIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Temperature [K] | 277 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1992-10-23 |
| Detector | WEISSENBERG |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 133.050, 147.460, 83.040 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.500 |
| R-factor | 0.206 |
| Rwork | 0.206 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 20.400 * |
| Data reduction software | BIOMOL |
| Data scaling software | WEIS |
| Phasing software | MLPHARE |
| Refinement software | TNT |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 10.000 | 2.670 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 47612 | |
| Completeness [%] | 83.1 | 53.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 294 | Kozlov, Y.Z., (1993) J. Mol. Biol., 232, 704. * |
