1DKK
BOBWHITE QUAIL LYSOZYME WITH NITRATE
Experimental procedure
| Detector technology | DIFFRACTOMETER |
| Collection date | 1989-05 |
| Detector | ENRAF-NONIUS FAST |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 28.000, 62.600, 60.800 |
| Unit cell angles | 90.00, 91.60, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.900 |
| R-factor | 0.157 * |
| Rwork | 0.157 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 25.000 * |
| Data reduction software | MADNES |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.900 * |
| Rmerge | 0.037 |
| Total number of observations | 43399 * |
| Number of reflections | 14910 |
| Completeness [%] | 85.0 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | sodium acetate | 5 (mM) | |
| 2 | 1 | drop | BWQL | 45 (mg/ml) | |
| 3 | 1 | drop | formamide | 0.625 (mM) | |
| 4 | 1 | drop | sodium nitrate | 6 (%(w/v)) | |
| 5 | 1 | reservoir | sodium acetate | 10 (mM) | |
| 6 | 1 | reservoir | formamide | 1.25 (mM) | |
| 7 | 1 | reservoir | sodium nitrate | 12 (%(w/v)) |
