1DIN

DIENELACTONE HYDROLASE AT 2.8 ANGSTROMS

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1987
Spacegroup name	P 21 21 21
Unit cell lengths	48.900, 71.450, 78.240
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.15 *
Rwork	0.150
RMSD bond length	0.014
RMSD bond angle	3.405 *
Data reduction software	XENGEN
Refinement software	PROLSQ

Data quality characteristics

	Overall
Rmerge	0.057
Number of reflections	29488
Completeness [%]	95.0
Redundancy	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.3 *	18 *	Pathak, D., (1988) J.Mol.Biol., 204, 435. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme
2	1	drop		0.86 (M)
3	1	reservoir		1.9 (M)