1DGW
Structure of the rhombohedral crystal of canavalin from jack bean
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1994-08-23 |
| Detector | SDMS |
| Spacegroup name | H 3 |
| Unit cell lengths | 136.876, 136.876, 76.004 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 500.000 * - 1.700 |
| R-factor | 0.192 |
| Rwork | 0.189 |
| R-free | 0.24500 * |
| RMSD bond length | 0.007 |
| RMSD bond angle | 25.500 * |
| Data reduction software | SDMS |
| Data scaling software | SDMS |
| Phasing software | MERLOT |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 300.000 | 1.780 |
| High resolution limit [Å] | 1.690 | 1.690 |
| Rmerge | 0.088 | 0.304 |
| Total number of observations | 343806 * | |
| Number of reflections | 56649 | 6947 * |
| <I/σ(I)> | 18.7 | |
| Completeness [%] | 95.0 | 81.1 |
| Redundancy | 6.1 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIQUID DIFFUSION | 6.8 | 293 | Koszelak, S., (1995) Biophys. J., 69, 13. * |
