1DGR
Refined crystal structure of canavalin from jack bean
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1989-01-23 |
| Detector | SDMS |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 136.500, 150.300, 133.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 500.000 * - 2.600 |
| R-factor | 0.181 * |
| Rwork | 0.180 |
| R-free | 0.22600 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 25.500 * |
| Data reduction software | SDMS |
| Data scaling software | SDMS |
| Phasing software | MERLOT |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 200.000 | 2.800 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.055 | 0.174 |
| Number of reflections | 37938 | |
| <I/σ(I)> | 21.3 | |
| Completeness [%] | 89.3 | 83 |
| Redundancy | 3.7 | 2.58 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.8 | 277 | Koszelak, S., (1995) Biophys. J., 69, 13. * |
