1DDT
THE REFINED STRUCTURE OF DIMERIC DIPHTHERIA TOXIN AT 2.0 ANGSTROMS RESOLUTION
Experimental procedure
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 105.640, 92.560, 65.580 |
| Unit cell angles | 90.00, 94.60, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.195 |
| Rwork | 0.195 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 2.600 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.5 * | 25 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG8000 | 12 (%(w/v)) | |
| 2 | 1 | reservoir | 0.43 (M) | ||
| 3 | 1 | reservoir | Tris-HCl | 0.043 (M) |
