1DCP

DCOH, A BIFUNCTIONAL PROTEIN-BINDING TRANSCRIPTIONAL COACTIVATOR, COMPLEXED WITH BIOPTERIN

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1995-09-29
Detector	RIGAKU
Spacegroup name	P 32 2 1
Unit cell lengths	105.700, 105.700, 196.170
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.300
R-factor	0.174 *
RMSD bond length	0.011 *
RMSD bond angle	2.300
Data reduction software	R-AXIS
Data scaling software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.300	2.300 *
Rmerge	0.057
Total number of observations	312481 *
Number of reflections	45971 *
Completeness [%]	78.0 *	39 *
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.4		ROOM TEMPERATURE, 1.7M AMSO4, 0.1M HEPES, PH 7.4