1DBQ

DNA-BINDING REGULATORY PROTEIN

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	38.040, 125.260, 61.290
Unit cell angles	90.00, 100.17, 90.00

Refinement procedure

Resolution	? - 2.200
R-factor	0.156 *
Rwork	0.156
RMSD bond length	0.018
RMSD bond angle	2.790
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	2.200 *	2.200 *
Rmerge	0.036 *
Number of reflections	25876 *
Completeness [%]	88.5 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	12 (mg/ml)
2	1	reservoir	PEG600	20 (%)
3	1	reservoir	Tris-HCl	0.1 (M)
4	1	reservoir		0.2 (M)