1DBA

THREE-DIMENSIONAL STRUCTURE OF AN ANTI-STEROID FAB' AND PROGESTERONE-FAB' COMPLEX

Experimental procedure

Spacegroup name	P 64 2 2
Unit cell lengths	134.760, 134.760, 124.210
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 2.800
R-factor	0.202
Rwork	0.202
RMSD bond length	0.018
RMSD bond angle	3.600
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000 *
High resolution limit [Å]	2.800 *
Rmerge	0.099 *
Number of reflections	17193 *
Completeness [%]	90.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	7.4 *	22 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	1.7 (M)
2	1	reservoir	PEG20000	0.002 (%(w/v))
3	1	reservoir	ethanol	1 (%(v/v))
4	1	drop	protein	5-25 (mg/ml)