1DB4
HUMAN S-PLA2 IN COMPLEX WITH INDOLE 8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1994-01-01 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 77.012, 77.012, 91.620 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.200 |
R-factor | 0.226 |
Rwork | 0.226 |
R-free | 0.25600 |
RMSD bond length | 0.009 |
RMSD bond angle | 24.330 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (98.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.240 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.069 | 0.286 |
<I/σ(I)> | 20.4 | 3.9 |
Completeness [%] | 95.6 | 94.2 |
Redundancy | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 297 | 10 MG/ML OF PROTEIN; 50 MM BUFFER (MES OR MOPS), 1% PYRIDINE, pH 7.0, VAPOR DIFFUSION, temperature 297K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | MES | 50 (mM) | or MOPS |
3 | 1 | drop | sodium chloride | 80-92 (%sat) | |
4 | 1 | drop | pyridine | 1 (%) |