1DAI

DETHIOBIOTIN SYNTHETASE COMPLEXED WITH 7-(CARBOXYAMINO)-8-AMINO-NONANOIC ACID

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-02-15
Detector	RIGAKU
Spacegroup name	C 1 2 1
Unit cell lengths	73.200, 49.200, 61.800
Unit cell angles	90.00, 107.10, 90.00

Refinement procedure

Resolution	6.000 - 1.640
R-factor	0.174
Rwork	0.174
RMSD bond length	0.013
RMSD bond angle	24.600 *
Data reduction software	R-AXIS
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.640 *
Rmerge	0.079
Number of reflections	19323
Completeness [%]	75.0
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *