1DAF
DETHIOBIOTIN SYNTHETASE COMPLEXED WITH 7-(CARBOXYAMINO)-8-AMINO-NONANOIC ACID, ADP, AND CALCIUM
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-02-26 |
Detector | RIGAKU RAXIS II |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 73.200, 49.200, 61.800 |
Unit cell angles | 90.00, 107.10, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.700 |
R-factor | 0.172 |
Rwork | 0.172 |
RMSD bond length | 0.014 |
RMSD bond angle | 24.200 * |
Data reduction software | R-AXIS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.700 * |
Rmerge | 0.059 |
Total number of observations | 52543 * |
Number of reflections | 21243 |
Completeness [%] | 93.0 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | cocrystallization * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | DAPA | 5 (mM) | |
2 | 1 | 1 | 200 (mM) | or 100mM MnCl2 |