1D99
STRUCTURAL FEATURES AND HYDRATION OF A DODECAMER DUPLEX CONTAINING TWO C.A MISPAIRS
Experimental procedure
Temperature [K] | 277 |
Detector technology | DIFFRACTOMETER |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.370, 41.440, 65.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.19 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 |
Number of reflections | 2452 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 * | 277 | referred to 'Wing, R..', (1980) 'Nature', 287, 755-758 * |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | MG ACETATE | ||
5 | 1 | 1 | SPERMINE | ||
6 | 1 | 2 | WATER |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | ||
2 | 1 | drop | magnesium acetate | ||
3 | 1 | drop | spermine hydrochloride molecule | ||
4 | 1 | reservoir | MPD | 20-30 (%) |