1D6F
CHALCONE SYNTHASE C164A MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 105 |
Detector technology | IMAGE PLATE |
Collection date | 1999-08-01 |
Detector | MACSCIENCE |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 97.768, 97.768, 65.228 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.450 - 1.690 |
Rwork | 0.182 |
R-free | 0.20100 |
RMSD bond length | 0.009 * |
RMSD bond angle | 2.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.730 |
High resolution limit [Å] | 1.690 | 1.690 |
Rmerge | 0.026 | 0.089 |
Total number of observations | 88359 * | |
Number of reflections | 39526 | |
<I/σ(I)> | 18.8 | |
Completeness [%] | 97.0 | 83.2 |
Redundancy | 2.2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 4 * | 2.2-2.4 M AMMONIUM SULFATE, 0.1 M BIS-TRIS PROPANE, 2 MM DITHIOTHREITOL (DTT), pH 6.5, VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 2.2-2.4 (M) | |
2 | 1 | reservoir | bis-Tris-propane | 0.1 (M) | |
3 | 1 | reservoir | dithiothreitol | 2 (mM) |