1CYI
CYTOCHROME C6
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1991-09 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 82.600, 82.600, 82.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.900 |
| R-factor | 0.197 |
| Rwork | 0.197 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.929 |
| Data reduction software | R-AXIS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 41.300 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.064 |
| Total number of observations | 19437 * |
| Number of reflections | 6412 |
| Completeness [%] | 84.8 |
| Redundancy | 3.03 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 8.8 (mg/ml) | |
| 2 | 1 | reservoir | Tris-HCl | 5 (mM) | |
| 3 | 1 | reservoir | PEG3350 | 25 (%) | |
| 4 | 1 | reservoir | 150 (mM) |
