1CTU
TRANSITION-STATE SELECTIVITY FOR A SINGLE OH GROUP DURING CATALYSIS BY CYTIDINE DEAMINASE
Experimental procedure
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 120.300, 120.300, 78.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.19 |
Rwork | 0.190 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.400 |
Data reduction software | R-AXIS |
Phasing software | X-PLOR (3.0) |
Refinement software | TNT (5A) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.082 * |
Total number of observations | 72498 * |
Number of reflections | 25451 |
Completeness [%] | 80.0 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.2 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 11-16 (mg/ml) | |
2 | 1 | drop | ammonium sulfate | 14-20 (%sat) | |
3 | 1 | reservoir | ammonium sulfate | 32-45 (%sat) |