1CTP

STRUCTURE OF THE MAMMALIAN CATALYTIC SUBUNIT OF CAMP-DEPENDENT PROTEIN KINASE AND AN INHIBITOR PEPTIDE DISPLAYS AN OPEN CONFORMATION

Experimental procedure

Spacegroup name	P 41 3 2
Unit cell lengths	171.500, 171.500, 171.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 2.900
R-factor	0.19
RMSD bond length	0.022
RMSD bond angle	4.300
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.900 *
Rmerge	0.097 *
Total number of observations	119740 *
Number of reflections	17821 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *			Knighton, D.R., (1991) Science, 253, 414. *