1CQA

BIRCH POLLEN PROFILIN

Experimental procedure

Source type	ROTATING ANODE
Temperature [K]	290
Detector technology	AREA DETECTOR
Collection date	1994
Detector	SIEMENS-NICOLET X100
Spacegroup name	P 41 21 2
Unit cell lengths	59.900, 59.900, 85.370
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.400
R-factor	0.178 *
Rwork	0.178
Structure solution method	SINGLE ISOMORPHOUS REPLACEMENT AND MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.025
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASES
Refinement software	PROFFT

Data quality characteristics

	Overall
Low resolution limit [Å]	30.100
High resolution limit [Å]	2.400
Rmerge	0.084 *
Number of reflections	5973
<I/σ(I)>	19.1
Completeness [%]	91.6
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6		pH 6.0

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	2.0 (M)
2	1	1	MES	100 (mM)