1CPC

ISOLATION, CRYSTALLIZATION, CRYSTAL STRUCTURE ANALYSIS AND REFINEMENT OF CONSTITUTIVE C-PHYCOCYANIN FROM THE CHROMATICALLY ADAPTING CYANOBACTERIUM FREMYELLA DIPLOSIPHON AT 1.66 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	180.260, 180.260, 61.240
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 * - 1.660
Rwork	0.181
RMSD bond length	0.016
RMSD bond angle	2.330
Refinement software	EREF

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.660 *	1.660 *
Rmerge	0.089 *
Total number of observations	176017 *
Number of reflections	70981 *
Completeness [%]		29.1 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	30 (mg/ml)
2	1	reservior	PEG	11 (%)
3	1	reservoir	phosphate	0.1 (M)