1CNR

CORRELATED DISORDER OF THE PURE PRO22(SLASH)LEU25 FORM OF CRAMBIN AT 150K REFINED TO 1.05 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	40.621, 18.345, 22.140
Unit cell angles	90.00, 91.03, 90.00

Refinement procedure

Resolution	? - 1.050
R-factor	0.105
RMSD bond length	0.022
RMSD bond angle	0.041
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.050 *	1.050 *
Number of reflections	14765 *	363 *
Completeness [%]	93.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *		20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein solution	30 (mg/ml)
2	1	drop	ethanol	80 (%(v/v))
3	1	reservoir	ethanol	60 (%)