1CNF

STRUCTURAL STUDIES ON CORN NITRATE REDUCTASE: REFINED STRUCTURE OF THE CYTOCHROME B REDUCTASE FRAGMENT AT 2.5 ANGSTROMS, ITS ADP COMPLEX AND AN ACTIVE SITE MUTANT AND MODELING OF THE CYTOCHROME B DOMAIN

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	145.200, 145.200, 47.500
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 2.700
R-factor	0.186
Rwork	0.186
R-free	0.27200
RMSD bond length	0.014
RMSD bond angle	27.900 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.700 *
Rmerge	0.062 *
Total number of observations	20157 *
Number of reflections	8225
Completeness [%]	81.0
Redundancy	2.4 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1