1CNE

STRUCTURAL STUDIES ON CORN NITRATE REDUCTASE: REFINED STRUCTURE OF THE CYTOCHROME B REDUCTASE FRAGMENT AT 2.5 ANGSTROMS, ITS ADP COMPLEX AND AN ACTIVE SITE MUTANT AND MODELING OF THE CYTOCHROME B DOMAIN

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	145.200, 145.200, 47.500
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 3.000
R-factor	0.19
Rwork	0.190
RMSD bond length	0.014
RMSD bond angle	27.700 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	3.000 *
Rmerge	0.101 *
Total number of observations	13089 *
Number of reflections	5737
Completeness [%]	76.0
Redundancy	2.3 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1