1CGL

Structure of the catalytic domain of fibroblast collagenase complexed with an inhibitor

Experimental procedure

Spacegroup name	P 64
Unit cell lengths	78.200, 78.200, 87.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	7.000 - 2.400
R-factor	0.186
Rwork	0.186
RMSD bond length	0.012
RMSD bond angle	2.200
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.067 *
Number of reflections	10896 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	PEG8000	15-30 (%(w/v))
2	1	1	ammonium sulfate	0.2 (M)
3	1	1	cacodylate	0.1 (M)