1C4G

PHOSPHOGLUCOMUTASE VANADATE BASED TRANSITION STATE ANALOG COMPLEX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	289
Detector technology	AREA DETECTOR
Collection date	1996-05-15
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	P 41 21 2
Unit cell lengths	174.420, 174.420, 101.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.700
R-factor	0.192
Rwork	0.192
R-free	0.29000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3pmg
RMSD bond length	0.023
RMSD bond angle	1.610
Data reduction software	XDS
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	X-PLOR (3.8)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.700
Number of reflections	36146
Completeness [%]	85.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1