1C4D
GRAMICIDIN CSCL COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Temperature [K] | 290 |
Detector technology | DIFFRACTOMETER |
Collection date | 1983-05 |
Detector | PICKER FACS-1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.118, 52.103, 31.174 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.000 |
R-factor | 0.232 |
Rwork | 0.232 |
Structure solution method | SINGLE WAVELENGTH ANOMALOUS SCATTERING FROM CESIUM |
RMSD bond length | 0.042 |
RMSD bond angle | 5.140 |
Data reduction software | HANSON (ET AL) |
Data scaling software | ANOSCL |
Phasing software | PHASIT |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.500 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 3813 | |
Completeness [%] | 99.8 | 99.2 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 25 MG/ML GRAMICIDIN IN 53 MM CSCL IN METHANOL AT 10C FOR 3 MONTHS, BATCH METHOD, TEMPERATURE 283K |