1BU7
CRYOGENIC STRUCTURE OF CYTOCHROME P450BM-3 HEME DOMAIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-03-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 59.380, 151.900, 62.770 |
| Unit cell angles | 90.00, 96.02, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.650 |
| R-factor | 0.197 |
| R-free | 0.25100 |
| Structure solution method | OTHER |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.023 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 1.690 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Number of reflections | 128585 | |
| <I/σ(I)> | 20.6 | 5.5 |
| Completeness [%] | 98.0 | 97.2 |
| Redundancy | 3.4 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7 | unpublished data. Journal is different from PDB file. * |
