1BQP
THE STRUCTURE OF THE PEA LECTIN-D-MANNOPYRANOSE COMPLEX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS II |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 73.926, 104.083, 64.837 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.100 |
| R-factor | 0.161 |
| Rwork | 0.161 |
| R-free | 0.18800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ltn |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.788 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.100 |
| Rmerge | 0.060 |
| Number of reflections | 27369 |
| Completeness [%] | 98.5 |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.0 |
